煤直接液化装置注硫系统优化分析

Optimization of sulfur injection system for coal direct liquefaction facility

  • 摘要: 煤直接液化装置采用液态硫作为硫化剂,将煤液化反应所用催化剂从饱和态转化为硫化态,以保证其催化活性。目前该装置注硫以高压注硫泵注入为主,催化剂浆混合罐底低压注硫为辅,因该高压注硫泵本体故障率较高且工艺操作条件苛刻,会出现注硫量不稳定、能耗高、维护成本高等问题,故需对注硫系统进行优化。从现有催化剂浆混合罐底低压注硫点引出管线,分别接至A、B、C三列油煤浆混合罐罐底,以四列低压注硫模式代替原催化剂浆混合罐底单线低压注硫,并适时停运高压注硫泵。结果表明,该优化措施在保障催化剂硫化及装置稳定运行的同时,节约设备运转及维护费用约57万元/年,并为后期同类煤制油化工项目工程设计提供参考。

     

    Abstract: Liquid sulfur is adopted in the coal direct liquefaction facility as a sulphide agent to convert the catalyst used in the coal liquefaction reaction from saturation to sulphide state to ensure its catalytic activity.At present, the sulfur injection is mainly injected by high pressure sulfur pump supplemented by low-pressure sulfur injection at the bottom of the catalyst slurry mixing tank.Due to the high failure rate of the high-pressure sulfur injection pump and the harsh process operation conditions, problems such as unstable sulfur injection, high energy consumption, and high maintenance costs have arisen, it is necessary to optimize the sulfur injection system.Pipeline is led out from the low-pressure sulfur injection point at the bottom of the existing catalyst slurry mixing tank and connected to the bottom of the oil-coal slurry mixing of the three series of A,B,C,replacing the original single-line low-pressure sulfur injection at the bottom of the catalyst slurry mixing tank with a four-series-pressure sulfur injection mode and stopping the high-pressure sulfur injection pump in due time.The optimization measure not only ensures the sulfonation and the stable operation of the facility but also saves about 570 000 yuan/year in equipment operation and maintenance costs.

     

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